![]() Bamboo Salt Which Contains Nephrite Jade Powder And Process For Preparing Thereof
专利摘要:
PURPOSE: A process for preparing bamboo salt with nephrite powder is provided, which has medical effects such as activation of cell functions and stimulation of blood circulation and metabolism, and can be also used as table salt. CONSTITUTION: The process for preparing bamboo salt with nephrite powder comprises the steps of: mixing 150-1000 mesh nephrite powder with 3-10 parts by weight of salt such as sun-dried salt, table salt, rock salt, regent grade sodium chlorite and potassium chlorite etc.; packing the mixture in a bamboo tube, which is prepared by cutting over three years old bamboo to form of tube with opened one side and clogged the other side; sealing the bamboo tube with 2mm thickness of yellow soil mud, which is prepared by mixing distilled water and yellow soil in a ratio of 3 : 7; putting the bamboo tubes in a fireplace with covering the bottom with pine tree and sprinkling with resin; heating at a temperature of over 900°C for 24 hours; taking out the bamboo salt and pulverizing to powder; putting the powder to the bamboo tube and heating again at a temperature of over 1500°C; and then making the bamboo salt to form of powder or particle. 公开号:KR20000060069A 申请号:KR1019990008106 申请日:1999-03-11 公开日:2000-10-16 发明作者:김준한 申请人:김준한;대일광업 주식회사; IPC主号:
专利说明:
Bamboo Salt Which Contains Nephrite Jade Powder And Process For Preparing Thereof} [10] The present invention relates to bamboo salt containing nephrite powder and a method for manufacturing the same, and in particular, by mixing a mixture of salt and nephrite powder in a bamboo barrel well and heating and dissolving it at a high temperature for a certain time, The present invention relates to bamboo salt containing nephrite powder, in which the nephrite powder immobilized in salt as a component acts as a main element for promoting metabolism of the human body, and a manufacturing method thereof. [11] In general, it is well known that jade or bamboo salt acts as a useful substance to the human body. The former jade is roughly divided into jadeite and jadeite, and jadeite is a lead fluoride mineral belonging to the pyroxene family. , Soda monoclinic system, hardness is a dense mass like crystal, light is black, cyan, green, transparent or translucent, and jade is generally called jadeite. Point. [12] Nephrite jade, on the other hand, is a monoclinic whiskey mineral of Inosilicates, and is divided into purgatory and serpentine superbasic purgatory among high-grade surrogate rocks, Their quality is determined by their fine structure, namely, the degree of fineness in which the hollow-tipped feldspar is made of fastening and fibers, and it is known that the finer the fiber, the better the quality. [13] According to a report published in the German authoritative medical literature ("KRAFF der KRISTALLE und der EDELSTEINE" by Mauda Palmer Die Verborgene), jadeite and purgatory are two different ores, which, like most gemstones, contain silicon and oxygen. While jadeite is formed of granular crystals, jadeite is composed of countless crystals and particulate aggregates such as fibers and hairs, and in this respect, jadeite is different from jadeite. Unlike the aluminum composition, it contains three minerals that are beneficial to the human body, namely calcium, iron, and magnesium, which have a great effect on the healing of diseases caused by hypertension, diabetic circulatory disorders, heart disease and kidney disorders. It was announced. [14] On the other hand, even in Dongbobogam, the classic medicine of oriental medicine, if you put jade into Omiju and Jiyuju, it turns into water, and if you put it in holjangsu, it is good to eat. When eaten at the same size as (체 大), the waste is discharged to the outside of the body, and 1 doeolsul and 1 yujicho (地 楡 草), 1 doe (稻米), 3 egret (白露) mixed together in a copper bowl When the rice is cooked, the oxol turns into water, which is called oxal (玉液) and is called Shinseonokjang (신농 옥장). Shinnongboncho, Dangboncho, and the main cortex According to the jade powder powder to make the enlightenment and taking it not only has the effect of moisturizing the five intestines and exhausting the waste in the body completely, ① it is effective in the digestive system by removing the heat in the stomach, ② Bronchial asthma, fever and heartburn It is good for severity and quenches thirst. ③ If you wear swelling clothes like sesame seeds, your body will fly and become lighter and longer. ④ It will help lubricate the lungs and help the vocal cords. ⑤ Nourishes the hair. It is said to nourish the function of the intestine, and especially to relieve stressful neurological disorders. It is known from the early days that rubbing the skin for a day, the main component of purgatory is consistent with the main elements of the human body and exerts an excellent effect on the human body without side effects. [15] On the other hand, bamboo and salt, which are the materials used for bamboo salt, contain ingredients such as cyanine, peonine, cyaninine, peonidine, galactose, etc., so that cell viability, tumors, cold symptoms, gum bleeding and It has been described as having excellent effect in the treatment of toothache and others. It is described in Dongbo Bogam, Herbal Wood, and New Herb, etc., and salt (sun salt, rock salt or sea salt) has been used for a long time because of the main ingredient "sodium chloride". It is used as a seasoning until it is an indispensable plant (食物) described in the above intentions Dongbobogam, herbaceous wood, new agricultural herb. That is to say more specifically, approximately 3% of the blood is a salt, this large amount of salt-free blood does not function. Equally important is that the gastric juice, which is indispensable for the digestion of all foods, depends on hydrochloric acid for its digestive power, and without salt in plants, digestion itself becomes impossible. Therefore, a normal adult should consume at least 10g of salt per day. [16] However, purgatory or bamboo salt has been used only for general purposes despite the excellent medical effects as described above. In particular, purgatory is known to have excellent medical effects, but due to its scarcity, it is only limited to some personal jewelry items such as necklaces, rings, and bracelets. [17] Therefore, the object of the present invention is to pay attention to the medical efficacy of the purgatory and bamboo salts as described above, and after many years of research experiments have been developed, and the mixture of salt and nephrite powder in an appropriate ratio is well ground in a bamboo barrel It is then sealed with ocher mud and heated and melted at a high temperature for a certain period of time, thereby purifying the medicinal properties of purgatory powder in addition to the bamboo salt properties, which contains the purgatory powder that promotes metabolism, promotes growth, and activates cellular functions. To provide a bamboo salt and a method for producing the same. [18] Bamboo salt containing the nephrite powder of the present invention to achieve the above object is characterized in that it contains 3 to 10% by weight of the nephrite powder in bamboo salt made by putting the salt into the bamboo barrel related to claim 1 and heating it. [19] The particle size of the nephrite powder is 150 to 1000 mesh, characterized in that the composition ratio (semi-quantitative analysis value (%)) as follows. [20] Silicon 34 [21] Magnesium 10 [22] Calcium 4.9 [23] Iron 0.23 [24] Aluminum 0.16 [25] Copper 0.17 [26] Cobalt 0.046 [27] Manganese 0.14 [28] Tin 0.024 [29] Beryllium 0.00072 [30] Is 0.0013 [31] Titanium 0.0038 [32] Nickel 0.0028 [33] Chromium 0.0030 [34] Miscellaneous 0 [35] In order to achieve the above object, the preparation method of bamboo salt containing purgatory powder of the present invention is filled with salt having a predetermined particle size in a bamboo barrel related to claim 3 and sealed as loess, which is a temperature of about 900 to 1500 ° C. for a predetermined time or more. In the bamboo salt manufacturing method of heat melting, coagulation and pulverization, characterized in that it comprises the step of mixing in the ratio of 3 to 10% by weight of the nephrite powder with a particle size of 150 to 1000 mesh. [36] The particle size of the nephrite powder is 150 to 1000 mesh in order to make the mixing with salt more homogeneous and stable. In addition, if the content of the purgatory powder is less than 3% by weight, it is not preferable because a stable effect due to the addition of the purgatory powder is not preferable. There is a possibility of lowering, so it is difficult to combine with salt, and the increase in product cost due to the high price of nephrite powder also occurs, so the maximum content is 10% by weight or less. [37] In preparing the salt, an ionic substance or the like beneficial to the human body may be optionally added. The nephrite powder used in the above is economically advantageous in terms of cost reduction because it is used to make products such as sculptures from the nephrite and to wash and finely grind the remaining residues. [1] 1 to 6 show the effect of purgatory used in the present invention on the cell growth of digitalis inana (Digitalis Ianata), [2] 1 is a graph showing the change in the total volume of the culture medium of the cells proliferating in the growth medium, [3] Figure 2 is a graph showing the change in cell volume, [4] Figure 3 is a graph showing the change in bio weight of cells, [5] 4 is a graph showing the change in dry weight of cells, [6] 5 is a graph showing the change in pH in cell growth medium, [7] 6 is a graph showing the change in pH of the production medium after the addition of purgatory powder, [8] 7 is a table showing the condition of the water analyzer containing the purgatory water used in the present invention, [9] 8 is a table showing the results of analysis of the water quality containing the purpura used in the present invention. [38] Hereinafter, a more preferred embodiment of the bamboo salt containing the purgatory powder according to the present invention and a manufacturing method thereof will be described in detail. [39] First, the nephrite powder having a particle size of 150 to 1000 mesh is mixed at a ratio of 3 to 10% by weight based on the previously prepared salt. At this time, the mixing means uses a general container mixer or a powder mixer. The mixture of salt and nephrite is well chopped into the inside of several bamboo barrels, one of which is blocked from the royal bamboo, which is about three years old and the other is cut open. The openings of the bamboo barrels are sealed to a thickness of approximately 20 mm using ocher mud made by mixing purified water and ocher in a ratio of approximately 3: 7. Bamboo barrels sealed with ocher mud are filled with pine in a clay furnace made of ocher and sprinkled with pine resin and then fired for at least 24 hours at 900 ℃ or higher. In this presbyopia, only the solidified bamboo salt pillars remain because the salt containing the purgatory powder, which absorbed gin such as bamboo and loess, is dissolved. After the inside of the furnace has cooled down, take out the bamboo salt lump containing purgatory pulverize it and crush it again and put it in a new bamboo barrel and repeat the fire as above. The temperature at this time is heated to about 1500 degreeC or more. Therefore, bamboo salt processed by primary is dissolved by bamboo gin by high temperature again, and when the fire is extinguished, the liquid hardens and turns like a lump of stone. This lump is a bamboo salt containing jade powder and can be pulverized as a powder or a predetermined granular form. [40] The salt is a natural salt, and in addition to the salt, rock salt, reagents, sodium chloride and potassium chloride are used. Bamboo or cotton bamboo is also used as bamboo, and the king bamboo, which is over 3 years old, is preferable. [41] <Example 1> [42] Mix the mixture of jade powder with a particle size of 150 mesh at a ratio of 3% by weight to salt, and chop it into a three-year bamboo barrel, seal it with ocher mud, and sequentially put it in a clay-made kiln. After heating and melting for more than hour, the solidified product was pulverized to obtain jade bamboo salt. [43] <Example 2> [44] Jade jade salt was obtained in the same manner as in Example 1 except that the nephrite powder having a particle size of 1000 mesh was mixed with the salt at a ratio of 10% by weight. [45] Bamboo salts are generally known to have detoxification, anti-blood effect, antibacterial action, and anti-inflammatory action, and therefore, the following experimental example described only the characteristics of nephrite powder mixed with bamboo salt on the human body. [46] <Experimental example 1> [47] In this experimental example, jade bamboo salt prepared in the above example and bamboo salt (containing no bamboo jade powder) prepared in the above example were examined for 50 men and women over 10 years old to examine the aesthetics of bamboo salt with added purgatory powder. In the range of about 10g or less so as not to know, according to the taste of each tester was eaten as it is eaten or dissolved in water to evaluate the aesthetics, the results are shown in Table 1 below. [48] Aesthetic characteristicsJade salt (the number of the respondents)Control Salt (Number of Respondents)I don't know (number of respondents) Gives a more refreshing taste28202 The salt is less bitter.30164 I feel a good fragrance25214 [49] As shown in the above experimental results, bamboo salt added with purgatory powder proved to be superior or comparable to the control bamboo salt in terms of consumers' taste. [50] <Experimental example 2> [51] The subjects of 50 adult men and women complaining of symptoms such as headache, numbness, indigestion, constipation, or diagnosed should continue to consume about 3 to 5 g of jade salt prepared in the above example for about 30 days. The effect was evaluated by. The results are shown in Table 2 below. [52] Effect Determination DiseaseNo effectEffectiveConsiderable effectCure effectsystem headache263One12 ConstipationOne75417 Urine34One412 IndigestionOne43One9 system7 (14%)21 (42%)12 (24%)10 (20%)50 (100%) [53] As shown in the above experimental results, the steady consumption of the jade bamboo salt of the present invention, headache (83%), constipation (94%), urinary tract pain (75%), indigestion (89%) is alleviated the effect as a dietary supplement It can be seen that there is. [54] <Experimental Example 3> [55] The following experimental examples test the presence of lead, heavy metals, and other toxic components in the jadeite added to the present invention. [56] <Lead content test> sampleJade minutes Sample propertyWhite powder Job numberFederal Institute of F.D.A.American Studies IW 091394-1 WayAtomic absorption analysis resultNot detected [57] <Heavy metal> sampleJade powder Sample propertyWhite Job numberFederal IW 080894-4 WayUSP 23 resultNot detected [58] <Inorganic elution test> sampleJade powder Sample propertyWhite Job numberFederal IW 080894-4 WayAs resultAs [59] 100 g of the sample was extracted with 1 liter of water by autoclave treatment, and the extract was analyzed. This is as follows. [60] AnalyteResults (ppm)Detection limit (ppm) Arsenic (As)ND0.05 Barium (Ba)ND0.20 Cadmium (Cd)0.0060.005 Chlorine (Cl)NDOne Chrome (Cr)ND0.01 Copper (Cu)ND0.05 FeND0.10 PbND0.05 Manganese (Mn)ND0.02 Mercury (Hg)ND0.0005 Nitrate (NO 3 )ND0.1 Selenium (Se)ND0.05 Silver (Ag)ND0.01 Sulfate (SO 4 )1.85One Zinc (Zn)ND0.01 [61] * ND = concentration is below or not detected [62] As shown in the above experimental results, the purgatory powder used in the present invention is free from harmful harmful lead, heavy metals, and other toxic components, and thus, stability when added to salt has been proved. [63] <Experiment 4> [64] In this experimental example, the experiment on the effect of the purgatory powder used in the preparation of the jade bamboo salt of the present invention for the experimental sphere (rabbit) was performed as shown in Table 7. [65] <Primary eye irritation test> sampleJade minutes Sample propertyMilky powder WayAs resultAs [66] Method: US Federal Register Vol 43.No 163-1978.8.22 p37359 [67] Experimental procedure: Place 0.1 ml of the extract on the inverted lower eyelid of one eye, and gently hold for 1 second before placing the upper and lower eyelids. The other eye is not treated and observed as a control example. The treated eyes of the six rabbits were left unwashed, and the eyes of the three rabbits were washed with running lukewarm water for one minute immediately after treatment. Prior to treatment with the sample, the eyes were examined in advance by fluorescence and only animals that did not show corneal damage were used for the test. Eye lesions were observed 24 hours, 48 hours, 72 hours, 7 days and 14 days after treatment. The results were shown in Table 8 below. [68] <Lesion degree of eyes> rabbittimeCorneal OpacityCorneal areaIris PriceConjunctival rednessConjunctival ChemosisConjunctival secretion # 1 fine24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) # 2 fine24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) # 3 fine24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) # 4 fine24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) # 5 fine24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) [69] # 6 fine24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) # 7wash24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) # 8wash24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) # 9wash24H000000 48H000000 72H000000 7D000000 scoreCorneal (0)Iris (0)Conjunctiva (0) [70] I. Cornea [71] (A) Opacity-Density (area for detoxification) [72] Normal-0 [73] Scattered Diffusion Zones-Details of the iris are clearly visible-1 [74] Translucent areas that are easily identified, slightly blurred details of the iris-2 [75] Milky white area, details of the iris are not visible, pupil size is almost indistinguishable [76] Opaque, no iris visible-4 [77] (B) corneal area [78] Normal-0 [79] Less than 1/4, but not 0-1 [80] More than 1/4, less than 1/2-2 [81] 1/2 or more, 3/4 or less-3 [82] More than 3/4, less than total area-4 [83] Score is A × B × 5, total max = 80 [84] II. Iris [85] (A) value [86] Normal-0 [87] Folded above normal, hyperemia, swelling, pericorneal congestion (these symptoms appear in any size, alone or in combination), the iris still responds to light (slow response is pronounced)-1 [88] Not responding to light, bleeding, total destruction (one or both of these symptoms)-2 [89] Score is A × 5, maximum possible total = 10 [90] III. conjunctiva [91] (A) red tide (only related to the conjunctiva of the eyelid) [92] Normal-0 [93] Blood vessels are surely reddened above normal-1 [94] More diffuse, deeper magenta, individual vessels not easily distinguished-2 [95] Spread red like beef-2 [96] (B) chemosis [97] No Snooze-0 [98] Random swelling phenomenon over normal (including eye blink membrane)-1 [99] Clearly swollen with partial inversion of the eyelids-2 [100] Eyelid half closed and swollen-3 [101] Eyelid half to full closed and swollen-4 [102] (C) secretion [103] Normal-0 [104] Any phenomenon other than normal (not including small amounts observed at the tip of the inner eye of normal animals)-1 [105] Secretions only on the eyelids and eyebrows adjacent to the eyelids-2 [106] Significant area around the eyes-3 [107] Score (A + B + C) × 2, total max = 20 [108] CONCLUSIONS: This sample was determined to be non-irritating to eyes, and therefore, it was found to be suitable for use in eye-related products. [109] <Primary skin irritation test> sampleJade minutes Sample propertyWhite powder WayAs resultAs [110] Method: US Federal Register Vol. 43, No. 163 [111] CTFA (The Cosmetic, Toiletry and Fragrance Association, Washington, D.C.) Technical Guidelines [112] Experimental procedure: Patch testing was performed on the skin of the white rabbit and the original skin. The hair was cut short at the back and sides. Two areas, about 10 cm away, were selected as patch locations. One area is made of four small epidermal incisions in the patch area (2 of which are tic-tac-toe vertically perpendicular to the other) and one-inch patches of surgical gauze. Is attached using a thin rubber band and adhesive tape. Samples are introduced into each site in amounts of 0.5 ml (g) under the patch. The body of the animal is wrapped with a rubberized cloth for 24 hours of exposure. The animal is immobile during the exposure time. After removing the patch, the results of evaluating the reactions at each site based on the scores described below were as follows. [113] Evaluation of Skin Response [114] Erythema and crust formation [115] No erythema-0 [116] Very weak erythema (recognizable barely)-1 [117] Properly identified erythema-2 [118] Moderate to severe erythema-3 [119] Severe erythema (beat red) to slight crust formation (deep damage)-4 [120] Edema [121] No edema-0 [122] Very mild edema (recognizable barely)-1 [123] Slight edema (it is obvious that the edges of the area are prominent)-2 [124] Moderate edema (approximately 1 mm up)-3 [125] result [126] rabbit24 hours72 hours Original skinWorn skinOriginal skinWorn skin EREDEREDEREDERED #One00000000 #200000000 # 300000000 #400000000 # 500000000 # 600000000 [127] Conclusions: This sample was determined to have no skin irritation. It has thus been found to be suitable for use in skin treatment products and the like. [128] <Acute oral toxicity [(0.5 g) / 100 g body weight] experiment> samplePurgatory powder Sample propertyWhite powder WayAs resultSame as Table 19 below [129] ratgenderInitial weight (g)Dosage (ml)Lag weight (g)Toxicity OneF2071.0219none 2F2111.1226none 3F2151.1225none 4F2081.0217none 5F2001.0213none 6M2271.1235none 7M2161.1224none 8M2051.0218none 9M2101.1224none 10M2121.1221none [130] Preparation of Samples: A portion of the sample was placed in sterile distilled water and boiled for 10 minutes to extract, and the extract was administered by intubation in an amount of 0.5 g per 100 g of body weight. [131] CONCLUSIONS: The sample meets the criteria for no oral toxicity. [132] <Experiment 5> [133] This experiment example is the process and result of the experiment performed by Inha University bio information system engineering laboratory to investigate the various effects of purgatory powder on the living body. [134] In this experiment, 70% of the constituent elements of the human body are water. Therefore, the impact of water on the water and the impact on the human body are investigated. Experiments on the effects were performed. [135] A. Hard water change [136] <Experiment 1> [137] 100 ml of artificially-made hard water was transferred to each of the four flasks by 50 ml, and purgatory was placed on the bottom of two flasks for about 10 minutes. [138] To determine the change in hardness, a titration method using ethylene diamineacetic acid (hereinafter referred to as "EDTA" titer 2.9412) was used. 1 ml of a buffer solution of pH 10, EBT was used as an indicator. [139] The change in hardness was measured by the amount of EDTA until the moment when the color of the hard water was changed by EDTA. At this time, the color returned to its original state over time, but in this experiment, the measurement was made based on the changing moment. [140] <Result 1> [141] At 100ppm of hard water, it takes 1.70ml of EDTA. [142] It takes 1.25ml of EDTA after purgatory test, so the hardness of 100.00ppm is lowered to 73.53ppm. That is, the hardness of 100.00 ppm was softened 26.47%. [143] <Experiment 2> [144] 200 ml of 100ppm hard water made in the same manner as in Experiment 1 was transferred to a beaker to immerse the purgatory. [145] After about 30 minutes, the water in the beaker was divided into three flasks to measure the change in hardness. In this experiment, the hardness was measured by adding EDTA until the color of hard water did not change any more after the color of hard water changed by EDTA. [146] <Result 2> [147] Each 100ppm hard water before purgatory experiment [148] 89.62 ppm [149] 91.19ppm [150] 89.62 ppm [151] Average 90.14ppm, thus 9.9% hardness decrease [152] <Experiment 3> [153] This experiment was conducted with tap water. Tap water was placed in a container and transferred to six flasks, and purgatory was placed at the bottom of three flasks, and hardness was measured after about 5 minutes. [154] <Result 3> [155] * Tap water without purgatory [156] 97.48 ppm [157] 97.48 ppm [158] 97.48 ppm [159] Average 97.48 ppm [160] * Tap water after purgatory experiment [161] 91.19ppm [162] 91.19ppm [163] 91.19ppm [164] Average 91.19ppm therefore, hardness decrease of 6.5% [165] I. Effect of Purgatory on the Proliferation of Digital Plant Suspensions of Digitalis lanata [166] ① Effect of Purgatory on the Growth of Digitalis lanata Cells in Growth Medium [167] 1 is a graph showing the change in the total volume of the culture medium of the cells proliferating in the growth medium for 11 days, Figure 2 is a graph showing the change in the cell volume, in proportion to the increase of the cells growing over time As the depletion of and the evaporation of the medium occur, the volume change of the whole culture reflects these factors. In particular, humidity and temperature in the atmosphere are closely related to the evaporation of the medium, and such factors also affect the cell growth rate. [168] As shown in the figure, the use of purgatory shows that the volume of the total culture solution is slightly decreased compared to the control group which is not used. This is because the use of purgatory rather than the control group has a faster cell growth rate against the evaporation of the medium or the depletion of nutrients, and thus, it is possible to offset the rapid decrease of the depleted medium to some extent. This phenomenon is observed in the case of continuous use of purgatory from day 4 to day 11 after inoculation of the cells as shown in Figure 2 measuring the volume change of the sunk cells only increase the volume of the cell than the unused control group This fact can be estimated. Therefore, the use of nephrite showed a faster cell growth rate than the control without the nephrite. These results can be said to be the result of delaying the decrease of the total volume than the control by offsetting the decrease in the total culture volume due to nutrient depletion and medium evaporation. In addition, the result of comparing the volume of the increased cell alone is also observed to show a tendency to gradually increase the cell volume after 4 days, it is thought that can support this result. [169] Cell proliferation and dry weight are the most common measures of cell proliferation. In general, the growth curve of all cells is represented by the S-shaped curve, which can be classified into four stages. Lag phase, which is a period of adaptation to the medium, in which there is no proliferation of cells and in which the mass does not increase. phase), the stationary phase, which has a maximum growth to some extent, and the Chinese food is slowed down and shows no mass increase, and the cell ruptures due to the depletion of nutrients, the release of toxic components, and the saturation of cell density. It can be divided into a dead phase where the total cell volume or mass decreases due to the tendency to die. [170] 3 and 4 are the results of measuring the cell biomass and dry weight. [171] 3 follows the growth curve of these four stages. In the case of using jade, after 7 days, the growth rate was slightly higher than that of the control without jade, and the growth stopped until 10 days, unlike the control showing the decrease in cell biomass. have. This is remarkable in that cell growth is continued even when the concentration of nutrient is almost depleted and the concentration in the medium becomes zero compared with the change in the concentration of glucose, a nutrient that acts as the main metabolic substrate in the medium. It is common to show a tendency to stop the growth and decrease the growth rate at the point of depletion of the influenced ingredients, like the control without purgatory, but the effect of purgatory on cell growth is different from purgatory It is assumed that there is. This result is also shown in Figure 4 after 3 days to show a cell growth proliferating at a higher rate than the control, and after 9 days the same phenomenon as in Figure 3. As a result, cells grown close to purgatory in growth media showed a better effect on cell growth than controls that did not. Digitalis lanata plant cells, which have a growth limit of about 10 days, are maintained in a stable state without cell necrosis without exchanging with new medium even after 10 days when cultured with purgatory. Rather, it is expected that cell proliferation may be an advantageous method for optimizing cell growth and concentration in the production process for the production of useful substances. [172] ② Effect of Purgatory on Changes in Medium pH [173] Figure 5 is a graph showing the pH change in the cell growth medium, Figure 6 is a graph showing the pH change of the production medium after the addition of purgatory powder. [174] Figure 5 is a measure of the change in pH of the medium in the case of using the purgatory in the growth medium and the control group not used. The control group shows a general tendency of pH in the medium applied to the plant cells, which gradually decreases over time and is maintained at a certain level. However, when using purgatory, it showed a similar trend to the control group until day 7, and gradually increased. This phenomenon is extreme in the result of FIG. 6 showing the result in the production medium in which the purgatory powder was added directly to the culture medium. . [175] The control group without added jade powder showed a consistent drop in pH, whereas the addition of jade powder showed a tendency to maintain the value to some extent. It is assumed that it acts as a cause. [176] ③ Results of analysis of water quality for purgatory [177] FIG. 7 is a table showing the condition of the water quality analyzer containing the nephrite powder used in the present invention, and FIG. 8 is a table showing the analysis results of the water quality containing the nephrite powder used in the present invention. [178] The data from FIGS. 7 and 8 are summarized in Table 13 to Table 16. Table 13 shows the measurement of each analysis item for Sample 1 after 48 hours in which 20 g of nephrite lump was added to the solution. In Table 13, there is almost no change in each measurement item, and the effect of purgatory is hardly seen. [179] Table 14 shows the measured values for each analysis item in Sample 2 after 48 hours of placing 20 g of purgatory lumps outside the solution. [180] Table 16 also shows the measured values for each analysis item in Sample 4 after 48 hours after placing the purge powder outside of the solution. However, in the case of Sample 3, the data measured for each analysis item of the sample 48 hours after 20 g of purgatory powder was added to the solution is shown in Table 15. There are many changes that can be seen in Table 15. The change is as follows. [181] Cr, Pb, Ni, and Co, which are harmful to the human body, changed significantly after 48 hours. Cr was removed in the absence of purgatory powder, that is, 45.30 mg before the reaction was removed to 0 after 48 hours in the purifying powder, and Pb was also completely removed from 13.76 mg to zero. Ni decreased from 51.8 mg to 1.733 mg and Co also decreased from 52.69 mg to 11.94 mg. [182] Mg, one of the necessary elements in the human body, increased from 48.36mg to 55.74mg. [183] The hydrogen ion concentration of distilled water was acidic to pH 3.5, but after the reaction, it was neutral to pH6.8, and the conductivity rapidly decreased. The adsorption force is physically large, about 3-4 mmol.q (equivalent) per gram. [184] Analytical results before and after the reaction in solution Purgatory lumps (purg of jade in solution) (Sample 1): Purgatory lumps in solution (20 g) ItemBefore the reactionAfter reaction (48hr)Change pH3.53.82- Ni51.8 mg51.75mg- Co52.69mg52.54mg- Cr45.30mg43.88mg- Mg48.36mg48.59 mg- Pb13.76 mg13.90mg- [185] Results of analysis of purgatory lumps outside the solution. (Sample 2): lump of purgatory jade (20g) ItemBefore the reactionAfter reaction (48hr)Change pH3.53.65- Ni51.8 mg48.92mg- Co52.69mg49.83mg- Cr45.30mg41.23mg- Mg48.36mg47.97mg- Pb13.76 mg15.1mg- [186] Analysis result when adding purgatory powder to the solution (Sample 3): Purgatory powder (20g) ItemBefore the reactionAfter reaction (48hr)Change pH3.56.8+3.3 Ni51.8 mg1.733 mg-50.06mg Co52.69mg11.94mg-40.75mg Cr45.30mg0mg-45.30mg Mg48.36mg55.74mg+ 7.38mg Pb13.76 mg0mg-13.76 mg [187] Analysis result when purgatory powder was placed outside the solution (Sample 4): Purgatory powder outside the solution (20g) ItemBefore the reactionAfter reaction (48hr)Change pH3.53.7- Ni51.8 mg51.53 mg- Co52.69mg52.55mg- Cr45.30mg43.0mg- Mg48.36mg48.39mg- Pb13.76 mg14.29 g- [188] As described above, the digitalis lanata plant suspension cells cultured for one week with nephrite close showed proliferation of about 30% or more without purgatory. This is a rare proliferative result even in the various experiments conducted for the proliferation effect on conventional Digigitalis lanata plant cells for high concentration culture. [189] In addition, experiments on how purgatory water affects hard water showed that soft water softened hard water without contact with water. [190] Particularly, in the component analysis experiments on water using distilled water, precipitation of nephrite was carried out. After 48 hours, in the component analysis, the pH was increased, the Ni and Co components were reduced, the Cr and Pb were removed, and the heavy metals were removed. An unusual phenomenon was observed that led to the phenomenon of. [191] As such, purgatory powder according to the present invention has not yet been clarified theoretically, but changes the hardness of water without contact with water, and also proliferates more than 30% of the digitalis innata plant suspension cells. The removal of heavy metals such as reduction of Ni, Co, Cr, Pb and other harmful substances is believed to be due to the radiation effect of the wavelength of the purgatory powder and the ionic reaction by minerals contained in the nephrite. These facts will be proved by the efficacy shown in the product of the present invention described above, and also the above experimental results in the case of jade bamboo salt containing the purgatory powder of the present invention due to the characteristics of salt and the effect of purgatory heavy metals This suggests that there will be effects such as removal of water, control of pH and softening of hard water. [192] As described above, according to the present invention, in addition to the intrinsic properties such as detoxification and antibacterial action by bamboo salt, synergistic medical properties of purgatory jade, in addition to the general effect of bamboo salt, as can be seen from the above experimental examples, Factors such as activation of water molecules, promotion of blood circulation, and activation of cell functions are generated, and have an excellent effect as a dietary supplement that promotes metabolism of the human body.
权利要求:
Claims (4) [1" claim-type="Currently amended] Bamboo salt containing bamboo jade powder, characterized in that it contains 3 to 10% by weight of jade jade powder in bamboo salt formed by heating and dissolving salt in a bamboo barrel and solidifying it. [2" claim-type="Currently amended] According to claim 1, wherein the grain size of the nephrite powder is 150 to 1000 mesh, bamboo salt containing the nephrite powder, characterized in that the composition ratio (semi-quantitative analysis value (%)) as follows. Silicon 34 Magnesium 10 Calcium 4.9 Iron 0.23 Aluminum 0.16 Copper 0.17 Cobalt 0.046 Manganese 0.14 Tin 0.024 Beryllium 0.00072 Is 0.0013 Titanium 0.0038 Nickel 0.0028 Chromium 0.0030 Miscellaneous 0 [3" claim-type="Currently amended] In the bamboo barrel filled with salt and sealed with loess mud, and heat-dissolved and solidified for a predetermined time at a temperature of approximately 900 to 1500 ℃, bamboo salt manufacturing method, A method for producing bamboo salt containing bamboo jade powder comprising the step of mixing the jade powder powder with a particle size of 150 to 1000 mesh at a ratio of 3 to 10% by weight based on the salt. [4" claim-type="Currently amended] The method according to claim 1, wherein the nephrite powder is composed of the following compositional ratio (semi-quantitative analysis value (%)). Silicon 34 Magnesium 10 Calcium 4.9 Iron 0.23 Aluminum 0.16 Copper 0.17 Cobalt 0.046 Manganese 0.14 Tin 0.024 Beryllium 0.00072 Is 0.0013 Titanium 0.0038 Nickel 0.0028 Chromium 0.0030 Miscellaneous 0
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同族专利:
公开号 | 公开日 KR100310160B1|2001-11-02|
引用文献:
公开号 | 申请日 | 公开日 | 申请人 | 专利标题
法律状态:
1999-03-11|Application filed by 김준한, 대일광업 주식회사 1999-03-11|Priority to KR1019990008106A 2000-10-16|Publication of KR20000060069A 2001-11-02|Application granted 2001-11-02|Publication of KR100310160B1
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申请号 | 申请日 | 专利标题 KR1019990008106A|KR100310160B1|1999-03-11|1999-03-11|Bamboo Salt Which Contains Nephrite Jade Powder And Process For Preparing Thereof| 相关专利
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